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Monosulfate was examined as a novel material for As(V) removal since its layered double hydroxide structure was expected to possess a high capacity for anion exchange. Phase-pure monosulfate was synthesized by hydration at 80–90°C for 36h using a stoichiometric mixture of tricalcium aluminate (calcined at 1300°C) and gypsum. The analyses of PXRD, WDXRF, and FE-SEM confirmed the successful synthesis...
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