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Anodic coupling of dithienylacetylene and dithienylacetylenes substituted with alkyl and alkoxy groups has been investigated in acetonitrile. The resulting polymers have been characterized by cyclic voltammetry, UV-Vis spectroscopy, electrochemical quartz crystal microbalance, in situ ESR and in situ conductivity. The degree of conjugation of the polymers is increased as the monomer oxidation potential...
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