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The new compounds LiLn9Mo16O35 (Ln=La, Ce, Pr, and Nd) were synthesized from stoichiometric mixtures of Li2MoO4, Ln2O3, Pr6O11 or CeO2, MoO3, and Mo heated at 1600 °C for 48 h in a molybdenum crucible sealed under a low argon pressure. The crystal structure, determined from a single crystal of the Nd member, showed that the main building block is the Mo16O36 unit, the Mo16 core of which is totally...
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