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Hierarchically structured 3D-Graphene nanosheets as supports for palladium nanoparticles (Pd/3D-GNS) were fabricated using the Sacrificial Support Method. The pore size distribution of the 3D-GNS supports were tuned by utilizing smaller and larger sized sacrificial silica templates, EH5 and L90. Using a combination of Scanning Electron Microscopy (SEM), N2 sorption and Rotating Ring Disc Electrode...
The electrooxidation of ethanol in alkaline media by palladium (Pd) nanoparticles supported on 3D-Graphene nanosheets with varying morphological and physicochemical properties was investigated using potentiodynamic and potentiostatic techniques. 30wt.% Pd electrocatalysts were synthesized using a surfactant-free soft alcohol reduction method (SARM) and deposited on thermally (7at.% H2, 800°C) and...
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