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Dilithium fluoride, Li-F-Li, has been produced in the gas phase by neutralization of the Li 2 F + cation, generated by fast atom bombardment ionization of lithium trifluoroacetate. Subsequent reionization after ~0.2 μs conclusively shows that the hypermetallic fluoride Li 2 F has survived intact and, thus, exists as a bound species. Charge reversal of Li 2 F + ...
Neutralization-reionization mass spectrometry is used to synthesize and identify in the gas phase the elusive aminocarbene, namely H-C-NH 2 . The carbene is prepared by reduction of the corresponding radical cation, generated by electron ionization of cyclopropyl amine. The mass spectrum obtained after subsequent reionization, about 0.2 μs later, confirms theoretical predictions that solitary...
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