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Oxidation of Fe–10Cr in dry and wet O 2 was studied at 600°C for up to 168h. Oxide microstructure was investigated by STEM/EDX, FIB/SEM and TEM. Oxidation in dry O 2 gives a Cr-rich protective (Fe 1−x Cr x ) 2 O 3 scale. The same protective oxide initially forms in O 2 +H 2 O environment, but after an incubation period scale breakdown...
This article focuses on the detailed microstructural investigation of the oxide scale formed on a 304 steel in the presence of oxygen and water vapour (40%) at 600°C. The work has been carried out using a combination of microanalytical techniques including FIB, TEM, EDX and electron diffraction. The local breakdown of the initially protective oxide scale and the growth of island/crater oxide morphology...
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