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Black single crystals of the new compounds Ba8Si2US14 and Ba8SiFeUS14 have been obtained by high-temperature solid-state methods at 1223 K. These isostructural compounds crystallize in a new structure type in space group C2h3 – C2/m of the monoclinic system. The salt-like structure comprises isolated US6 octahedra and MS4 tetrahedra separated by Ba cations. The US6 octahedra form pseudo-layers that...
Single crystals of Cs 3 Ln 7 Te 12 (Ln = Sm, Gd, Tb) have been grown accidentally through the reaction of Ln and Te with a CsCl or Cs 2 Te 3 flux at elevated temperatures. The crystal structures have been determined from single crystal X-ray diffraction data. These compounds, which are isostructural with Rb 3 Yb 7 Se 12 , crystallize...
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