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N,N′-diisobutyloxycarbonyl-N″,N‴-(1,3-propylene)-bisthiourea (L) and its silver(I) and gold(I) complexes were designed and synthesized. Treatment of 1,3-propanediamine with the isothiocyanate iPrCH2OC(O)NCS yielded bisthiourea L with over 90% yield. Treatment of L with AgNO3 in CH3CN afforded coordination polymer {[Ag(L)(NO3)·CH3CN]}n (1) with layer structure, while with HAuCl4 in CH3CN resulted in...
4,4′,4″-[1,3,5-Benzenetriyltris(carbonylimino)]trisbenzoic acid (H 3 L), a C 3 -symmetric ligand, was found to self-assemble into an interesting core-rosette structure driven by intermolecular hydrogen-bonding interactions. Reactions of this ligand with Zn 2+ , Co 2+ and Cd 2+ under solvothermal conditions resulted in the formation of four new coordination polymers...
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