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We have studied the high spin and low spin structural phases of the two-step spin transition compound [Fe(bpp) 2 ](NCS) 2 ·2H 2 O (bpp: 2,6-bis(pyrazol-3-yl)pyridine) of different sample history with X-ray synchrotron (λ∼0.32Å) powder diffraction at different temperatures as well as with usual X-ray (λ∼1.54Å) powder diffraction at room temperature by performing rapid repeated...
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