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Metal hexacyanoferrates are well known molecular solids for a large variety of cations, although very little has been described for actinide adducts. Two new members of actinide(III) hexacyanoferrates were synthesized with the cations americium and californium. They were structurally characterized by infrared and X‐ray absorption spectroscopy. Combined EXAFS data at the iron K edge and actinide L3...
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