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Well crystallized Fe-based oxyhydroxy-fluoride with the FeO(OH 0.2 F 0.8 )·0.2H 2 O chemical composition has been prepared from hydrolysis of Fe trifluoride under supercritical CO 2 conditions. Investigation by Mössbauer spectroscopy and neutron diffraction show that this compound crystallize in the monoclinic symmetry (SG: I2/m, a=10.447(7)Å, b=3.028(2)Å, c=10.445(4)Å,...
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