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Mechanically alloyed Fe 75 Nb 5 Ge 20 alloys have been studied using different TEM techniques. For short milling times the microstructure of the system consists of an inhomogeneous mixture of the starting crystalline phases: small bcc Fe nanocrystallites, filament-like bcc Nb and spherical fcc Ge. After long milling times, the microstructure consists of a single bcc supersaturated...
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