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The role of ligands (i.e. hexadecylamine, dodecylamine, or octylamine associated with oleic acid) on the formation of ZnO nanoparticle superlattice structures (NSSs) was investigated by NMR spectroscopy in C7D8. This full study demonstrates that ion‐paired ammonium carboxylates play a crucial role in NSS formation. Using different NMR spectroscopic experiments, such as 1H NMR, pulsed field gradient...
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