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Glass‐ceramics are possible host matrix for high level waste immobilization. The Gd2Zr2O7 glass‐ceramic matrix was successfully synthesized using spark plasma sintering (SPS) method in 5 minutes. The phase transition with sintering temperature was studied using X‐ray diffraction, Raman and transmission electron microscopy. It revealed that samples kept a main defected fluorite phase as being sintered...
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