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Defluorination of PTFE by alkyllithium/electron-donating solvents such as N,N,N',N'-tetramethylethylenediamine (TMEDA), hexamethylphosphoramide (HMPA) was studied by means of spectroscopy such as ESR, 7 Li- and 13 C-NMR, XPS, UV-Vis and IR. Based on the experimental results, it was concluded that an electron from radical species, which was generated in the alkyllithium/electron-donating...
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