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In article number 1902321, Claus Feldmann and co‐workers present the formation of zero‐valent iron nanoparticles (Fe0) by lithium pyridinyl‐driven reduction of FeCl3 (Fe+III) in pyridine and their subsequent use as reactive starting material to obtain FeCp*2 (Fe+II, Cp*: pentamethylcyclopentadienyl). The novel pyridine‐based synthesis of reactive Fe0 nanoparticles as well as further follow‐up reactions...
The synthesis of zero‐valent iron (Fe(0)) nanoparticles in pyridine using lithium bipyridinyl ([LiBipy]) or lithium pyridinyl ([LiPy]) is presented. FeCl3 is used as the most simple starting material and reduced either in a [LiBipy]‐driven two‐step approach or in a [LiPy]‐driven one‐pot synthesis. High‐quality nanoparticles are obtained with uniform, spherical shape, and mean diameters of 2.9 ± 0...
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