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Cotton-extracted cellulose nanocrystals are spin-coated from aqueous suspension (0.6wt%) onto glass slides to give ca. 40nm thick films. Impregnation with LiCl and redox active Fe(CN)63−/4− into this film gives extremely thin redox active layers (typically 170nm at 60% relative humidity), which were investigated with a 4-point or 3-point probe electrochemical system based on 250μm diameter platinum...
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