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Nickel‐rich layered transition metal oxides, LiNi1−x(MnCo)xO2 (1−x ≥ 0.5), are appealing candidates for cathodes in next‐generation lithium‐ion batteries (LIBs) for electric vehicles and other large‐scale applications, due to their high capacity and low cost. However, synthetic control of the structural ordering in such a complex quaternary system has been a great challenge, especially in the presence...
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