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A total synthesis of the proposed structure of the natural macrolactone phomolide G (1) by a bidirectional strategy from L‐tartaric acid is reported. The ω‐terminus of the molecule was elaborated by nitrile extension, C3‐alkylation and a substrate‐controlled 1,3‐ketone reduction. The α‐terminus was extended by a C2 aldehyde‐to‐alkenal homologation followed by an auxiliary controlled aldol reaction...
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