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Nanosized Ni–Al LDHs were synthesized via a hydrothermal method by using Au colloidal nanoparticles as nuclei for LDH growth, designated as Au/Ni–Al LDHs. Transmission electron microscopy, X-ray diffraction and X-ray photoelectron spectroscopy were used to characterize the structure and morphology. N2 physisorption was performed to measure the specific surface area. Electrochemical impedance spectroscopy...
This paper reports the fabrication of Au nanoparticles (Au NPs)‐Ni‐Al layerd double hydroxide (LDH) composite film by one step electrochemical deposition on the surface of a glass carbon electrode from the mixture solution containing HAuCl4 and nitrate salts of Ni2+ and Al3+. Improved conductivity was obtained by Au NPs codeposited on LDH film. The synergic effect of LDHs and Au NPs dramatically improves...
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