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A mixture of elemental Ga and Se with the nominal composition Ga 40 Se 60 was submitted to the Mechanical alloying technique and their structural, thermal and optical properties were followed by X-ray diffraction, differential thermal analysis, photoacoustic spectroscopy, UV–VIS‐NIR absorbance spectroscopy and Raman spectroscopy techniques. After 10h of milling the X-ray pattern showed...
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