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The formation of Zn0.6Co0.4Fe2O4 spinel-based pigments by sol–gel method and post-annealing pathway and the impact of polyol structure on their properties were investigated. The phase evolution and mass changes of gels during annealing were assessed by thermal analysis. The differential thermal analysis revealed that above 400 °C the carboxylate precursors decompose to ZnFe2O4, CoFe2O4, and Zn2SiO...
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