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The most accurate measurements of the mass attenuation coefficient for metals at low temperature for the zinc K‐edge from 9.5 keV to 11.5 keV at temperatures of 10 K, 50 K, 100 K and 150 K using the hybrid technique are reported. This is the first time transition metal X‐ray absorption fine structure (XAFS) has been studied using the hybrid technique and at low temperatures. This is also the first...
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