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The effect of nanoconfinement on the equilibrium free radical polymerization of methyl methacrylate (MMA) is investigated using differential scanning calorimetry. The ceiling temperature is shifted to lower temperatures in 13 nm diameter pores, with pore surface chemistry showing no significant effect. The results indicate that the change in the entropy of propagation decreases in nanopores due to...
The effect of nanoconfinement on the free radical polymerization of methyl methacrylate (MMA) is investigated using differential scanning calorimetry, gel permeation chromatography, and 1H nuclear magnetic resonance. Both hydrophobic and hydrophilic 13 nm-diameter controlled pore glasses (CPG) are used for polymerization under nanoconfinement. The number-average and weight-average molecular weights...
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