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1,1,4,4‐Tetramethyl‐2‐tetrazene (TMTZ) as a hypergolic nontoxic prospective alternative was prepared and characterized by elemental analysis. The highest yield and purity can be obtained at the experimental parameters (UDMH/NH2Cl ratio 3:1; reaction time 20 min; extraction 15 min by ether, room temperature), in which the overall molar yield of TMTz is over 90%, with a purity up to 98.8%. The detailed...
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