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Copper sulfides were synthesized through a fast and simple subcritical and supercritical methanol technique by controlling the reaction temperature. CuS and Cu9S5 microcrystals with different particle sizes and morphologies were prepared. The composition, morphology, and structure of the products were analyzed using XRD, SEM, TEM, DLS, XPS, and FTIR. UV–vis was used to investigate their optical behaviors...
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