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Revealing the photocatalytic mechanism between various junctions and catalytic activities has become a hotspot in photocatalytic systems. Herein, an internal molecular heptazine/triazine (H/T) junction in crystalline carbon nitride (HTCN) is constructed and devoted to selective two‐electron oxygen reduction reaction (2e− ORR) for efficient hydrogen peroxide (H2O2) production. In‐situ X‐ray diffraction...
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