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The microstructure of the α-Fe/Nd 2 Fe 14 B nanocomposite magnets prepared by electropulsing heating amorphous Nd 8 Fe 84 Co 3 B 5 has been studied by employing X-ray diffraction (XRD) and transmission electronic microscopy (TEM). The grain size d of the α-Fe phase keeps almost invariable, e.g., d≈18–19 nm, with the increase of its volume fraction during...
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