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The article shows how additional information can be obtained from coupling a self constructed DTA-system with a commercially available BRUKER D8 DISCOVER GADDS XRD2-microdiffractometer. The dehydration process of gypsum to anhydrite in the temperature range from room temperature up to 723 K is used as an example. Due to the short measurement times of 10 s for each diffraction pattern the three phase...
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