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A novel nanoparticulate polyacetylene-supported Pd(II) catalyst (NP-Pd(II)) for use in the aqueous Suzuki-Miyaura cross coupling reaction was successfully synthesized by simply treating an aqueous solution of PdCl42– with acetylene under ambient conditions. Electron microscopy, Fourier transform infrared spectroscopy, Raman spectroscopy, X-ray diffraction, X-ray photoelectron spectroscopy and X-ray...
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