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The salt Na 2 [Rh 12 (CO) 30 ] was used for the hydroformylation of 2,4,4-trimethyl-1-pentene in tetrahydrofuran under high pressures of CO/H 2 (20-120 atm) in the temperature range 300-400 K. The reaction is highly chemioselective, approaching 100% selectivity to 3,5,5-trimethylhexanal, and only traces of 2,4,4-trimethylpentane and 3,5,5-trimethyl-l hexanol...
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