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As a new type of high‐entropy material, most of the current work has focused on the synthesis and characterization of mechanical properties of high‐entropy diboride ceramics (HEBs). In this work, single‐phase HEBs with 5–9 cations were prepared by spark plasma sintering with self‐synthesized HEB powders through the boro/carbothermal reduction method. The distribution of the metal elements in the obtained...
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