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The surface structure of a Pd layer electrochemically deposited onto Au(111) from PdCl 2-4 solution has been studied by surface X-ray diffraction. By combining the measurements of the specular and non-specular rod profiles, both in-plane and out-of-plane structures have been determined. On the Au(111) electrode surface, Pd occupies the cubic closest packing site and forms a pseudomorphic...
When a platinum electrode is dipped into aqueous sulfuric acid solution containing Formaldehyde, the surface is covered by CO, which is formed by the dissociative adsorption of formaldehyde. A second harmonic generation voltammogram pumped by a 532 nm laser pulse and photo-reflectance voltammogram probed by a 670 nm laser beam are sensitive to the surface CO and surface oxide, respectively. The experiments...
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