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In this work three alloys, Fe74Nb6B20, Fe64Ni10Nb6B20 and Fe54Ni20Nb6B20, were obtained by mechanical alloying to analyze the influence of Ni content on Fe–Nb–B alloy formation. Structural analysis by X-ray diffraction (XRD) confirms that partial substitution of Fe by Ni favours the formation during milling of a more disordered structure. Furthermore, thermal stability study was performed by differential...
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