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Herein, we report a series of CuPd catalysts for electrochemical hydrogenation (ECH) of furfural to 2‐methylfuran (MF or FurCH3 where Fur=furyl) in aqueous 0.1 M acetic acid (pH 2.9). The highest faradaic efficiency (FE) for MF reached 75 % at −0.58 V vs. reversible hydrogen electrode with an average partial current density of 4.5 mA cm−2. In situ surface‐enhanced Raman spectroscopic and kinetic isotopic...
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