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The synthetic Mg–Al hydrotalcite with Mg/Al molar ratio of 2 was hydrothermally treated in autoclaves under autogenous water vapour pressure at 120–200 °C for 2–18 h. The obtained samples were characterized by powder X-ray diffraction (XRD), scanning electron microscopy (SEM) and surface area measurements. A well-crystallized hydrotalcite-like phase was present in the coprecipitated product. No other...
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