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Millerite NiS nanocrystals have been prepared through the solvent (hydro-) thermal method. The XRD patterns indicated that the products were pure millerite NiS with cell parameters a=9.624(4) Å, c=3.150(1) Å. Using ethylenediamine and hydrazine hydrate as solvent resulted in the formation of rod-like nanocrystalline NiS, whereas spherical nanoparticles were obtained using aqueous ammonia as solvent...
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