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Cobalt phosphides and lithiated cobalt phosphides are prepared by high-energy ball-milling at room temperature. With increasing the milling time, the phosphide structure is converted from CoP3 to CoP phase. The initial electrochemical lithiation of CoPx (CoP3+CoP) and CoP leads to a reversible capacity of 878 and 533 mAh/g. The faradic yield at the first cycle is about 74% for both the samples. Partial...
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