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Ni 2 P/SiO 2 was pretreated with a 0.8% H 2 O–99.2% H 2 flow at 303, 514, and 543 K. The Ni 2 P/SiO 2 catalysts before and after treatment were characterized by N 2 adsorption-desorption, X-ray diffraction, inductively coupled plasma atomic emission spectrometry, H 2 temperature-programmed desorption, and in situ diffuse reflection infrared...
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