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A fluoride-ion conductor, γ-PbSnF4, was synthesized by the mechanical milling. In addition, β-PbSnF4 was obtained by aging the γ-PbSnF4 at 473K. The electrical conductivity of β-PbSnF4 is relatively higher than that of γ-PbSnF4 at 298K. The crystal structure analysis of γ- and β-PbSnF4 was carried out using neutron diffraction data. From the obtained occupancies, fluoride ions were located at the...
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