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A novel restricted access material was prepared by surface initiated atom transfer radical polymerization. The bi‐layer‐polymer structures were created on the surface of silica layer‐by‐layer. The inner layer was composed of poly(styrene‐co‐divinylbenzene), which was grafted first for binding small molecules based on hydrophobic and π–π interactions. The poly(styrene‐co‐divinylbenzene) bonded silica...
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