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Catalytic oxidation of toxic organic pollutants in water urgently requires improved efficiency for practical application. Here a wrapping‐pyrolysis strategy is exploited to convert CoP nanowires‐threaded ZIF‐8 into CoP nanoparticles‐confined nitrogen‐doped yolk‐shell porous carbon polyhedra, featuring high‐density active sites, and high adsorbability, dispersibility and conductivity (4‐High). The...
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