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A novel silylene supported iron hydride [Si, C]FeH (PMe3)3 (1) was synthesized by C (sp3)‐H bond activation with zero‐valent iron complex Fe (PMe3)4. Complex 1 was fully characterized by spectroscopic methods and single crystal X‐ray diffraction analysis. To the best of our knowledge, 1 is the first example of silylene‐based hydrido chelate iron complex produced through activation of the C (sp3)−H...
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