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K n C 60 (THF) m (n = 1-3, m = n) have been prepared via solution-phase route. Variable temperature 13 C NMR data reveal that there exists a strong correlation of 13 C NMR chemical shift with the degree of orientational order of C 60n- in these materials. The implications of this observation to the origin of down-field chemical...
NaC 60 (THF) 3 has been prepared via a new solution-phase route. The solid-state variable temperature ESR and 13 C NMR studies on NaC 60 (THF) 3 (in comparison with NaC 60 (THF) 5 ) suggest that the unusual down-field chemical shift in C 60- (relative to C 60 ) can be understood partially on...
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