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This work is concerned with the dissolution of cellulose in tetraallylammonium fluoride/DMSO; the thermal stability of electrolyte solution, and relevant mechanistic aspects of the biopolymer acylation. EMF measurements (fluoride ion-selective electrode) showed that the electrolyte is present as monohydrate. 1 H NMR spectroscopy showed that it does not undergo elimination via ylide intermediate,...
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