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A series of Mo3VOx/H4SiW12O40/Al2O3 catalysts were prepared and applied to one-step oxydehydration of glycerol to acrylic acid. The catalysts were thoroughly characterized by BET, XRD, TEM, TGA, NH3-TPD, and XAFS techniques. It was found that acetic acid was produced in parallel with acrylic acid with similar yield when adjusting Mo3VOx content in the catalysts. Increasing calcination temperature...
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