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We review structures of high-density CO monolayers on Pt(111) surfaces in CO-saturated electrolytes or in gaseous CO at near atmospheric pressure, using surface X-ray scattering (SXS) and scanning tunneling microscopy (STM). In electrolytes, we confirmed the well-known (2×2)-3CO and (√19×√19)-13CO structures and were able to study the transition between them. For gas-phase studies, we were able to...
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