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Two mono iron complexes Fe(CO)2PR3(NN) (R = Cy (3), Ph (4), NN = o-phenylenediamine dianion ligand, N2H2Ph2–) derived from the ligand substitution of Fe(CO)3I2PR3 by the NN ligand were isolated and structurally characterized by single crystal X-ray diffraction. They have a similar first coordination sphere and oxidation state of the iron center as the [Fe]-hydrogenase active site, and can be a model...
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