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To gain insight into which parameters control the hydrolytic stability of the silane multilayer at the silica-matrix interface, the effects of addition of hydrochloric acid to silane solution on the characteristics of silane adsorbed on to a colloidal silica surface were investigated using g.p.c. and CP/MAS 29 Si n.m.r. The characteristics of the silane chemisorbed on the silica surface in...
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