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The results of three experimental studies, i.e. GC‐MS of peroxide‐cross‐linked alkene/alkane mixtures, 13C NMR of peroxide‐cured, 13C‐labeled 2‐ethylidene‐5‐norbornene ‐ ethylene‐propylene‐diene‐monomer (EPDM) and EPR of peroxide curing of EPDM, are combined, yielding a more accurate description of the mechanism of peroxide cure of EPDM. Both alkyl and allyl macro‐radicals are formed via H‐abstraction...
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